A Green and Efficient Solvothermal Liquid-Phase Exfoliation Method for Synthesizing ZnO Nanorods as Electrodes in Supercapacitors

Document Type : Review Article

Author

Department of Inorganic Chemistry, Faculty of Sciences, Masaryk University, Kotlárská 2, 611 37 Brno, Czech Republic

10.22091/jaem.2025.3808

Abstract

This work presents a straightforward, eco-friendly, and effective approach for fabricating ZnO nanorods to be used as electrode materials in electrochemical supercapacitors. The nanorods were synthesized through a novel solvothermal liquid-phase exfoliation technique, leveraging the unique properties of double hydroxides. The structural and morphological characteristics of the synthesized ZnO nanorods were thoroughly examined using X-ray diffraction (XRD) and scanning electron microscopy (SEM), respectively. Electrochemical performance tests of the modified electrodes were conducted in a three-electrode setup using an electrochemical workstation. The results demonstrated a pseudocapacitive behavior with a high specific capacitance of 135.23 F/g at a current density of 1 A/g in a 1 M Na2SO4 electrolyte, indicating that these nanostructures are promising candidates for supercapacitor electrode applications.

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